Publicación:
Desarrollo de materiales compuestos reforzados basados en fibras de carbono recicladas modificadas con nanoalambres: caracterización, conformación y evaluación mediante nanoindentación

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dc.contributor.advisorCantero Guevara, Miriam Elenaspa
dc.contributor.advisorMeléndrez Castro, Manuel Franciscospa
dc.contributor.authorEsquivel Galarcio, Samir Enriquespa
dc.date.accessioned2023-02-10T14:29:27Z
dc.date.available2023-02-10T14:29:27Z
dc.date.issued2023-02-09
dc.description.abstractLos materiales compuestos reforzados con fibras de carbono (CFRP), presentan excelentes propiedades mecánicas, debido a sus elevadas propiedades específicas, por esto cada día están siendo implementados por diversos sectores industriales, como el aeroespacial, automotriz, marino, entre otros. Lo que genera un aumento en los residuos de este material, los cuales son eliminados mediante dos métodos no sostenibles, los vertederos y la incineración. Una solución a esta problemática consiste en reciclar estos materiales, sin embargo, luego del reciclaje existe una reducción de las propiedades al usar fibras de carbono recicladas (rCF), como la pérdida de resistencia a la tracción y la poca adherencia entre el material reciclado y la nueva matriz. El objetivo de este trabajo es desarrollar CFRP, incorporando nanorods de ZnO alineados verticalmente sobre rCF, para mejorar la interfase resina-fibra y de esta manera mejorar las propiedades mecánicas del material compuesto. Las rCFs se modificaron superficialmente por oxidación ácida (HNO3), posteriormente se hicieron crecer nanorods de ZnO utilizando el proceso por vía húmeda. Luego, fueron funcionalizadas con APTES (3-aminopropiltrietoxisilano) mediante el proceso de hidrolisis para mejorar la interacción físico/química con la matriz epoxi. Las fibras fueron caracterizadas mediante la microscopía electrónica de barrido (SEM), microscopía electrónica de transmisión (TEM), microscopía de fuerza atómica (AFM), espectroscopia ultravioleta-visible (UV-V), difracción de rayos X (DRX), espectroscopia Raman y espectroscopia infrarroja (FT-IR). Por último, se evaluaron las propiedades mecánicas de todas las fibras mediante una prueba de tracción al compuesto y nanoindentación. En la caracterización estructural Raman, se aprecia que la relación 𝐼𝐷/𝐼𝐺, son de 2.037 para las rCF-P-NRDs ZnO y 2.066 para rCF-M-NRDs ZnO, lo que indica que hay un menor daño morfológico respecto a las rCF de control, afirmando que el crecimiento indujo en la recuperación de las fibras. Por otro lado, según los resultados SEM, se puede hacer crecer nanorods de ZnO alineados verticalmente sobre rCF mediante la reacción por vía húmeda, obteniendo diámetros de 179.642 nm. Por último, los valores obtenidos mediante los ensayos de tracción indicaron que hubo una mejora del 45% (rCF-P-NRDs ZnO) y 56% (rCF-M-NRDs ZnO) respecto a la fibra de carbono virgen.spa
dc.description.degreelevelPregradospa
dc.description.degreenameQuímico(a)spa
dc.description.modalityTrabajos de Investigación y/o Extensiónspa
dc.description.tableofcontents1. INTRODUCCIÓN. ................................................................................................... 1spa
dc.description.tableofcontents2. HIPÓTESIS .............................................................................................................. 4spa
dc.description.tableofcontents3. OBJETIVOS ............................................................................................................. 4spa
dc.description.tableofcontents3.1. Objetivo General ................................................................................................ 4spa
dc.description.tableofcontents3.2. Objetivos Específicos ........................................................................................ 4spa
dc.description.tableofcontents4. ESTADO DE ARTE. ................................................................................................ 5spa
dc.description.tableofcontents4.1. Fibras de Carbono. ............................................................................................. 5spa
dc.description.tableofcontents4.1.1. Precursores para obtener fibras de carbono. ............................................... 6spa
dc.description.tableofcontents4.1.2. Demanda mundial de las fibras de carbono. ............................................... 9spa
dc.description.tableofcontents4.2. Materiales Compuestos. ................................................................................... 11spa
dc.description.tableofcontents4.2.1. Tipos de matrices poliméricas. ................................................................. 11spa
dc.description.tableofcontents4.3. Propiedades Mecánicas. ................................................................................... 14spa
dc.description.tableofcontents4.3.1. Tracción al Compuesto. ............................................................................ 15spa
dc.description.tableofcontents4.3.2. Nanoindentación. ...................................................................................... 15spa
dc.description.tableofcontents4.4. Reciclaje de Fibras de Carbono. ...................................................................... 16spa
dc.description.tableofcontents4.4.1. Tipos de reciclaje. ..................................................................................... 17spa
dc.description.tableofcontents4.4.2. Recuperación de rCF a partir de modificaciones superficiales. ............... 20spa
dc.description.tableofcontents5. METODOLOGÍA. .................................................................................................. 27spa
dc.description.tableofcontents5.1. Modificación superficial de Fibras de Carbono con HNO3 ............................. 27spa
dc.description.tableofcontents5.2. Síntesis de nanopartículas de ZnO. .................................................................. 28spa
dc.description.tableofcontents5.3. Crecimiento de Nanorods de ZnO. .................................................................. 30spa
dc.description.tableofcontents5.4. Funcionalización amínica de fibras de Carbono con Nanorods de ZnO ......... 32spa
dc.description.tableofcontents5.5. Fabricación del material compuesto. ............................................................... 33spa
dc.description.tableofcontents5.5.1. Caracterización de material compuesto. ................................................... 33spa
dc.description.tableofcontents6. RESULTADOS Y DISCUSIÓN DE RESULTADOS. .......................................... 35spa
dc.description.tableofcontents6.1. Modificación superficial con HNO3 ................................................................ 35spa
dc.description.tableofcontents6.1.1. Resultados FT-IR. ..................................................................................... 35spa
dc.description.tableofcontents6.1.2. Resultados Raman. ................................................................................... 37spa
dc.description.tableofcontents6.2. Síntesis de Nanopartículas de ZnO .................................................................. 41spa
dc.description.tableofcontents6.2.1. Resultados UV-Visible. ............................................................................ 41spa
dc.description.tableofcontents6.2.2. Resultados de Microscopia de fuerza atómica AFM. ............................... 41spa
dc.description.tableofcontents6.3. Crecimiento de Nanorods de ZnO alineados verticalmente en fibras de carbono recicladas. ................................................................................................................... 43spa
dc.description.tableofcontents6.3.1. Resultados de Microscopia Electrónica de Barrido SEM y Microscopia Electrónica de Trasmisión (TEM). ......................................................................... 43spa
dc.description.tableofcontents6.3.2. Resultados de Difracción de Rayos X (DRX). ......................................... 46spa
dc.description.tableofcontents6.3.3. Resultados Raman. ................................................................................... 49spa
dc.description.tableofcontents6.4. Funcionalización amínica de fibras de carbono recicladas con nanorods de ZnO. 52spa
dc.description.tableofcontents6.4.1. Resultados FT-IR. ..................................................................................... 52spa
dc.description.tableofcontents6.4.2. Resultados Raman. ................................................................................... 53spa
dc.description.tableofcontents6.5. Fabricación del Material Compuesto. .............................................................. 55spa
dc.description.tableofcontents6.5.1. Resultados de tracción al compuesto. ....................................................... 55spa
dc.description.tableofcontents6.5.2. Resultados de Nanoindentación................................................................ 60spa
dc.description.tableofcontents7. CONCLUSIONES .................................................................................................. 63spa
dc.description.tableofcontents8. REFERENCIAS BIBLIOGRAFICAS ................................................................... 64spa
dc.format.mimetypeapplication/pdfspa
dc.identifier.urihttps://repositorio.unicordoba.edu.co/handle/ucordoba/7062
dc.language.isospaspa
dc.publisher.facultyFacultad de Ciencias Básicasspa
dc.publisher.placeMontería, Córdoba, Colombiaspa
dc.publisher.programQuímicaspa
dc.rightsCopyright Universidad de Córdoba, 2023spa
dc.rights.accessrightsinfo:eu-repo/semantics/embargoedAccessspa
dc.rights.creativecommonsAtribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)spa
dc.rights.urihttps://creativecommons.org/licenses/by-nc-nd/4.0/spa
dc.subject.keywordsAcid oxidationeng
dc.subject.keywordsZnO Nanorods,eng
dc.subject.keywordsFunctionalizationeng
dc.subject.proposalOxidación ácidaspa
dc.subject.proposalNanorods de ZnOspa
dc.subject.proposalFuncionalizaciónspa
dc.titleDesarrollo de materiales compuestos reforzados basados en fibras de carbono recicladas modificadas con nanoalambres: caracterización, conformación y evaluación mediante nanoindentaciónspa
dc.typeTrabajo de grado - Pregradospa
dc.type.coarhttp://purl.org/coar/resource_type/c_7a1fspa
dc.type.contentTextspa
dc.type.driverinfo:eu-repo/semantics/bachelorThesisspa
dc.type.versioninfo:eu-repo/semantics/submittedVersionspa
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