Publicación:
Caracterización química, física y mecánica de materiales compuestos con matriz de ácido poliláctico y refuerzo particulado de cáscaras de marañón elaborados a través de la técnica de moldeo por deposición fundida

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dc.contributor.advisorEspitia Sanjuán, Luis Armandospa
dc.contributor.advisorColorado Lopera, Henry Alonso
dc.contributor.authorPaternina reyes, María José
dc.date.accessioned2023-02-25T19:10:28Z
dc.date.available2024-02-24
dc.date.available2023-02-25T19:10:28Z
dc.date.issued2023-02-22
dc.description.abstractIn this work, composite materials with polylactic acid matrix were made, varying the percentages of cashew shell particles 0.5%, 1% and 2% using the fused deposition molding (FDM) technique; The cashew shells were dried at 250ºC and crushed mechanically, using particles with a size smaller than 63 um to manufacture them. Polylactic acid and cashew shells were characterized by FTIR, scanning electron microscopy, thermogravimetric analysis, lignocellulosic analysis, and for the composite materials obtained, mechanical tests were carried out to obtain tensile and flexural mechanical properties according to ASTM D638 and ASTM D790 standards, In addition to the analyzes of the fractures obtained in each test. It was found that the shell has the presence of hemicellulose, cellulose and lignin, in addition to other minerals present in smaller quantities. The drying process at 250ºC managed to eliminate the anacardic acid present in the cashew shell. It was evidenced that the composite materials with 0.5% cashew shell particles had higher values of modulus of elasticity and tensile strength, however, in the yield stress, the 1% composite materials presented the highest properties. On the other hand, in bending, an increase in bending resistance was observed as the percentage of added particles increased.eng
dc.description.degreelevelMaestríaspa
dc.description.degreenameMagíster en Ingeniería Mecánicaspa
dc.description.modalityTrabajos de Investigación y/o Extensiónspa
dc.description.resumenEn este trabajo se realizaron materiales compuestos con matriz de ácido poliláctico variando los porcentajes de partículas de cáscara de marañón 0.5%, 1% y 2% mediante la técnica de moldeo por deposición fundida (FDM); las cáscaras de marañón fueron secadas a 250ºC y trituras de forma mecánica utilizando para la fabricación de estos mismo, las partículas con tamaño menor de 63 um. El ácido poliláctico y las cáscaras de marañón fueron caracterizados mediante FTIR, microscopia electrónica de barrido, análisis termogravimétrico, análisis lignocelulósicos y para los materiales compuestos obtenidos se desarrollaron ensayos mecánicos para obtener propiedades mecánicas a tensión y flexión acorde a las normas ASTM D638 y ASTM D790, además de los análisis de las fracturas obtenidas en cada ensayo. Se encontró que la cáscara tiene presencia de hemicelulosa, celulosa y lignina, además de otros minerales presentes en menor cantidad, El proceso de secado a 250ºC logró eliminar el ácido anacárdico presente en la cáscara de marañón. Se evidenció que los materiales compuestos con 0.5% de partículas de cáscaras de marañón tuvieron mayores valores de módulo de elasticidad y resistencia a tensión, no obstante, en el esfuerzo a fluencia los materiales compuestos de 1% presentaron las mayores propiedades. Por su parte en flexión se vio un incremento en la resistencia a flexión a medida que se aumentaba el porcentaje de partículas añadidas.spa
dc.description.tableofcontentsRESUMEN ...................................................................................................................... 7spa
dc.description.tableofcontentsABSTRACT..................................................................................................................... 8spa
dc.description.tableofcontents1. Capítulo I. Descripción del trabajo de investigación .......................................... 9spa
dc.description.tableofcontents1.1. INTRODUCCIÓN............................................................................................................9spa
dc.description.tableofcontents1.2. Objetivos. .......................................................................................................................11spa
dc.description.tableofcontents1.2.1. Objetivo general................................................................................................................ 11spa
dc.description.tableofcontents1.2.2. Objetivos específicos. ...................................................................................................... 11spa
dc.description.tableofcontents1.3. Estructura de la tesis....................................................................................................12spa
dc.description.tableofcontents1.4. Revisión de literatura....................................................................................................13spa
dc.description.tableofcontents1.4.1. Materiales compuestos.................................................................................................... 13spa
dc.description.tableofcontents1.4.2. Marañón (Anacardium Occidentale).............................................................................. 14spa
dc.description.tableofcontents1.4.3. Moldeo por deposición fundida (FDM) .......................................................................... 18spa
dc.description.tableofcontents1.5. Trabajos derivados .......................................................................................................22spa
dc.description.tableofcontents2. Capítulo II. DISEÑO DE EXPERIMENTOS............................................................23spa
dc.description.tableofcontents2.1. Materiales y métodos ...................................................................................................23spa
dc.description.tableofcontents2.1.1. Hipótesis............................................................................................................................. 23spa
dc.description.tableofcontents2.1.2. Universo ............................................................................................................................. 23spa
dc.description.tableofcontents2.1.3. Variables ............................................................................................................................ 23spa
dc.description.tableofcontents2.1.4. Recolección de datos....................................................................................................... 24spa
dc.description.tableofcontents3. Capítulo III: Caracterización de materiales .........................................................27spa
dc.description.tableofcontents3.1. Introducción ...................................................................................................................27spa
dc.description.tableofcontents3.2. Materiales y métodos. ..................................................................................................28spa
dc.description.tableofcontents3.3. Resultados.....................................................................................................................30spa
dc.description.tableofcontents3.4. Conclusiones .................................................................................................................40spa
dc.description.tableofcontents4. Capítulo IV. Obtención de filamentos..................................................................41spa
dc.description.tableofcontents4.1. Introducción. ..................................................................................................................41spa
dc.description.tableofcontents4.2. Materiales y métodos. ..................................................................................................42spa
dc.description.tableofcontents4.3. Resultados .....................................................................................................................43spa
dc.description.tableofcontents4.4. Conclusiones .................................................................................................................49spa
dc.description.tableofcontents5. Capítulo V. Obtención de Materiales compuestos .............................................50spa
dc.description.tableofcontents5.1. Introducción ...................................................................................................................50spa
dc.description.tableofcontents5.2. Materiales y métodos. ..................................................................................................51spa
dc.description.tableofcontents5.3. Resultados .....................................................................................................................54spa
dc.description.tableofcontents5.4. Conclusiones .................................................................................................................58spa
dc.description.tableofcontents6. Capítulo VI. Medición de propiedades mecánicas .............................................59spa
dc.description.tableofcontents6.1 Introducción ...................................................................................................................59spa
dc.description.tableofcontents6.2.1. Ensayo de tensión ................................................................................................................ 59spa
dc.description.tableofcontents6.2.2. Ensayos de flexión................................................................................................................ 60spa
dc.description.tableofcontents6.3. Resultados ........................................................................................................................61spa
dc.description.tableofcontents6.4. Conclusiones ....................................................................................................................77spa
dc.description.tableofcontents7. Conclusiones Generales y futuros trabajos .......................................................78spa
dc.description.tableofcontents7.1. Futuros trabajos. ...........................................................................................................78spa
dc.description.tableofcontents8. Bibliografía.............................................................................................................80spa
dc.description.tableofcontents9. Anexos ...................................................................................................................88spa
dc.format.mimetypeapplication/pdfspa
dc.identifier.urihttps://repositorio.unicordoba.edu.co/handle/ucordoba/7225
dc.language.isospaspa
dc.publisher.facultyFacultad de Ingenieríaspa
dc.publisher.placeMontería, Córdoba, Colombiaspa
dc.publisher.programMaestría en Ingeniería Mecánicaspa
dc.rightsCopyright Universidad de Córdoba, 2023spa
dc.rights.accessrightsinfo:eu-repo/semantics/embargoedAccessspa
dc.rights.creativecommonsAtribución-NoComercial-SinDerivadas 4.0 Internacional (CC BY-NC-ND 4.0)spa
dc.rights.urihttps://creativecommons.org/licenses/by-nc-nd/4.0/spa
dc.subject.keywordsCashew shelleng
dc.subject.keywordsComposite materialeng
dc.subject.keywordsAgroindustrial wasteeng
dc.subject.keywordsMechanical propertieseng
dc.subject.keywordsFDMeng
dc.subject.proposalCascara de marañónspa
dc.subject.proposalMaterial compuestospa
dc.subject.proposalresiduo agroindustrialspa
dc.subject.proposalPropiedades mecánicasspa
dc.subject.proposalFDMspa
dc.titleCaracterización química, física y mecánica de materiales compuestos con matriz de ácido poliláctico y refuerzo particulado de cáscaras de marañón elaborados a través de la técnica de moldeo por deposición fundidaspa
dc.typeTrabajo de grado - Maestríaspa
dc.type.coarhttp://purl.org/coar/resource_type/c_bdccspa
dc.type.contentTextspa
dc.type.driverinfo:eu-repo/semantics/masterThesisspa
dc.type.redcolhttps://purl.org/redcol/resource_type/TMspa
dc.type.versioninfo:eu-repo/semantics/submittedVersionspa
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